Applied biomechanics to evaluate the properties of laser beam treated orthopedic implants
Description
Laser beam marking is used to ensure biomaterials' identification and traceability. The texturing imparts greater adhesion to the surfaces of implantable medical devices. The aim of this work was to evaluate the surface behaviour of the austenitic stainless steel ABNT NBR ISO 5832-1 marked and textured by optical fiber laser beam using selected parameters, changing the pulse frequency; in face of its biomechanical behaviour, through tests of tensile strength, fatigue and wear; verify the localized corrosion susceptibility by electrochemical tests in a solution that simulates the body fluids; and analyze microstructural changes. The treatments performed altered the biomaterials roughness and their micro hardness as a function of the increase of the pulse frequency. The microstructure and chemical composition of the surfaces underwent changes that directly affected the passive layer of the stainless steels, triggering the corrosion process. This effect was evidenced by SVET, XPS and characterization of electronic properties of the passive film by the Mott-Schottky technique. These two types of laser treatments increased the surfaces' magnetic susceptibility. The parameters used for the marking and texturing did not induce a decrease in the cellular viability of the samples, as no cytotoxicity was showed even after prolonged incubation. This biomaterial was adequate on the biomechanical tests, since the laser treatments, under the conditions used, did not induce the formation of surface tensions of magnitude capable of leading the fatigue fracture, indicating infinite fatigue life; the region of fracture by tension could not be related to the laser marking. The wear volume decreased as a function of the increase in micro hardness produced by the increase of the pulse frequency in the texturing. The visual character of the markings and texturing was assured after the majority of the tests performed. (author)
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Additional details
Additional titles
- Original title (Portuguese)
- Biomêcanica aplicada na avaliação de propriedades de implantes ortopédicos metálicos tratados por feixe laser
Publishing Information
- Imprint Pagination
- 204 p.
- Report number
- INIS-BR--19620
INIS
- Country of Publication
- Brazil
- Country of Input or Organization
- Brazil
- INIS RN
- 49015724
- Subject category
- S36: MATERIALS SCIENCE;
- Resource subtype / Literary indicator
- Thesis
- Descriptors DEI
- AUSTENITIC STEELS; BIOLOGICAL MATERIALS; CORROSION; FATIGUE; IMPLANTS; LASER RADIATION; MICROSTRUCTURE; TENSILE PROPERTIES; TEXTURE; WEAR; X-RAY PHOTOELECTRON SPECTROSCOPY
- Descriptors DEC
- ALLOYS; CARBON ADDITIONS; CHEMICAL REACTIONS; ELECTROMAGNETIC RADIATION; ELECTRON SPECTROSCOPY; IRON ALLOYS; IRON BASE ALLOYS; MATERIALS; MECHANICAL PROPERTIES; PHOTOELECTRON SPECTROSCOPY; RADIATIONS; SPECTROSCOPY; STEELS; TRANSITION ELEMENT ALLOYS