Published June 2002
| Version v1
Report
Determination of rhenium in environmental samples by ICP-MS
Description
A simple separation method for Re determination in rock and seawater samples by inductively coupled plasma mass spectrometry (ICP-MS) has been developed. An extraction chromatographic resin (TEVA resin, Eichrom Ind. Inc.) was employed to separate Re from sample matrices and trace elements that cause isobaric interference during ICP-MS measurements. Total average yields were 94±3% for rock and soil samples and almost 100% for water samples. The method was applied to trace-level Re determination in standard igneous rock and seawater samples. The measured Re values were 0.05 - 4.0 ng/g for the rock samples and 6.3 - 12.7 pg/mL for the seawater samples. (author)
Additional details
Publishing Information
- Imprint Title
- Proceedings of the third workshop on environmental radioactivity
- Imprint Pagination
- 300 p.
- Journal Page Range
- p. 57-62
- Report number
- KEK-PROC--2002-7
Conference
- Title
- 3. workshop on environmental radioactivity
- Dates
- 5-7 Mar 2002
- Place
- Tsukuba, Ibaraki (Japan)
INIS
- Country of Publication
- Japan
- Country of Input or Organization
- Japan
- INIS RN
- 34004261
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Resource subtype / Literary indicator
- Conference, Non-conventional Literature
- Descriptors DEI
- ENVIRONMENTAL MATERIALS; EXTRACTION CHROMATOGRAPHY; ICP MASS SPECTROSCOPY; ION EXCHANGE MATERIALS; RESINS; RHENIUM; ROCKS; SEAWATER; SEPARATION PROCESSES; SOILS
- Descriptors DEC
- CHROMATOGRAPHY; ELEMENTS; HYDROGEN COMPOUNDS; MASS SPECTROSCOPY; MATERIALS; METALS; ORGANIC COMPOUNDS; ORGANIC POLYMERS; OXYGEN COMPOUNDS; PETROCHEMICALS; PETROLEUM PRODUCTS; POLYMERS; REFRACTORY METALS; SEPARATION PROCESSES; SPECTROSCOPY; TRANSITION ELEMENTS; WATER
Optional Information
- Notes
- 15 refs., 2 figs., 2 tabs.