Published June 1988 | Version v1
Journal article

Acetylene insertion and thermolysis reactions of [η4-catena(PhAs)8] [Mo2(CO)6]. The synthesis and crystal structure of [(PhAs)8Mo2 (CO)6] [C2CO2CH3]2 and ([Mo(CO)4]2) (μ-Ph2AsAsPh) (μ-Ph2As)

  • 1. Delaware Univ., Newark (USA). Dept. of Chemistry

Description

Reactive acetylenes are inserted at one (but not both uncoordinated As-As bonds to form an enlarged, but structurally related complex. The second molybdenum complex is formed with dimethylacetylene carboxylate and the third by thermolysis at 1500C. Crystal structures are determined. 5 refs

Additional details

Publishing Information

Journal Title
New Journal of Chemistry
Journal Volume
12
Journal Issue
6-7
Series
New J. Chem.
Journal Page Range
565-570
ISSN
0398-9836
CODEN
NJCHD

INIS

Country of Publication
France
Country of Input or Organization
France
INIS RN
20014804
Subject category
S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
Descriptors DEI
BOND ANGLE; BOND LENGTHS; CHEMICAL PREPARATION; CRYSTAL STRUCTURE; MOLECULAR STRUCTURE; MOLYBDENUM COMPLEXES
Descriptors DEC
COMPLEXES; SYNTHESIS; TRANSITION ELEMENT COMPLEXES