Published April 23, 2018 | Version v1
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Experimental and numerical studies on the micromechanical crystal plasticity behavior of an RPV steel

Description

The PhD project studies the mechanical response of the reactor pressure vessel steel A508cl3 (or 16MND5 in French nomenclature) at the microscopic scale by experimental analyses and numerical simulations. Different aspects of in-situ tests inside an SEM chamber have been considered. First, the characterization and corrections of bias and uncertainties of different SEM imaging modalities (SE, BSE, and EBSD) have been performed. Precise registrations of SEM images in different modalities have been developed in order to give a comprehensive description of the sample surface topographies. Crystallographic orientation maps (from EBSD analyses) are registered to measure the crystal rotation and displacement fields along the tensile test. The elastic deformations of the surface are assessed by integrated correlation of high-resolution electron diffraction images. The 3D microstructure of the analyzed sample is revealed a posteriori by combining FIB milling and EBSD images. The experimental test is also simulated by crystal plasticity calculations on a 3D mesh created according to the 3D microstructure observed in the deformed configuration. An algorithm has been proposed to estimate its initial configuration and to identify the plastic parameters iteratively. A synthetic 2D model has been used to prove its feasibility. Two crystal plasticity laws have been validated on the 3D mesh, namely dislocation dynamics for body-centered cubic crystals and a modified version of Meric-Cailletaud model. In the present work finite element model updating was used to provide two sets of parameters (for ferrite and bainite) for the latter law. (author)

Abstract (French)

Cette these vise a etudier le comportement mecanique de l'acier de cuve 16MND5 (ou A508cl3 pour la norme anglaise) a l'echelle de la microstructure en croisant des approches experimentale et numerique. Plusieurs contributions au developpement de l'essai de traction in-situ a l'interieur de MEB ont ete apportees. En premier, les biais de mesure de differentes modalites (BSE, EBSD et SE) d'acquisition d'images sous MEB ont ete caracterises et corriges. Les images MEB de differentes modalites ont ete correlees de facon precise afin de decrire la topographie de l'eprouvette. Les images d'orientation cristallographique (EBSD) ont ete correlees afin de reveler la rotation cristalline et les champs de deplacement de surface au long de la traction. La deformation elastique de l'eprouvette a ete mesuree par correlation integree des images de diffraction electronique a haute-resolution. Les microstructures fines de l'eprouvette a trois dimensions apres deformation ont ete mesurees par FIB-EBSD. L'essai a egalement ete simule par calcul de plasticite cristalline sur un maillage 3D, base sur les microstructures mesurees dans la configuration deformee. Un algorithme a ete propose pour estimer la configuration initiale de l'eprouvette et identifier les parametres de loi de plasticite en procedant par iterations. Un cas test synthetique 2D a ete employe pour valider la faisabilite de l'algorithme. Deux lois de plasticite cristalline ont ete testees sur le maillage 3D: dynamique des dislocations des cristaux cubiques centres, et une version modifiee de la loi Meric-Cailletaud. Pour cette derniere loi, deux jeux de parametres ont ete identifies pour les ferrites et bainites par recalage des elements finis. (auteur)

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Additional details

Additional titles

Original title (English)
Etudes experimentales et numeriques de plasticite cristalline d'un acier de cuve

Publishing Information

Imprint Pagination
327 p.
Report number
FRNC-TH--12544

Optional Information

Notes
[290 refs.]; Available from the INIS Liaison Officer for France, see the INIS website for current contact and E-mail addresses