Published April 1995 | Version v1
Journal article

Structure of Co(2), Ni(2) and VO(2) complexes with 4-phenylthiosemicarbaziddiacetic acid

  • 1. AN Moldavskoj SSR, Kishinev (Moldova, Republic of). Inst. Khimii
  • 2. AN Moldavskoj SSR, Kishinev (Moldova, Republic of). Inst. Prikladnoj Fiziki

Description

Structure of complex compounds VO(2)(3) with 4-phyenylthiosemicarbaziddiacetic acid is determined through X-ray diffraction method. Monocrystal compounds are monoclinic, sp.gr. P21/n (a=6.703(2), b=12.470(7), c=1695(6) A, γ=95.10(4) deg). The organic molecule in the complexes is expressed in form of twofold deprotonated tetradentate, ligand joining to metal according to the tripod type with application of donor atoms S, N, O, O and forming three metallocycles. The coordination surrounding of the central atom is supplemented by one oxygen vanadyl atom and one water molecule. 17 refs.; 4 figs.; 5 tabs

Additional details

Additional titles

Original title (Russian)
Stroenie kompleksnykh soedinenij Co(2), Ni(2) i VO(2) s 4-feniltiosemikarbaziddiuksusnoj kislotoj

Publishing Information

Journal Title
Koordinatsionnaya Khimiya
Journal Volume
21
Journal Issue
4
Journal Page Range
p. 341-348.
ISSN
0132-344X
CODEN
KOKHDC