Published March 1987
| Version v1
Journal article
Synthesis of U-14C-labelled 5-hydroxymethyl-2-furaldehyde
Description
Uniformally 14C-labelled 5-hydroxymethyl-2-furaldehyde was synthesized by dehydration of D-[U-14C]fructose on an H+ ion exchange resin and a water isobutylmethyl ketone biphasic liquid reaction medium. The optimal reaction time was 45 min, and after HPLC purification the radiochemical yield was 50%. The whole process took 2 hours. (author)
Additional details
Publishing Information
- Journal Title
- J. Labelled Compd. Radiopharm.
- Journal Volume
- 24
- Journal Issue
- 3
- Series
- J. Labelled Compd. Radiopharm.
- Journal Page Range
- 343-348
- ISSN
- 0362-4803
- CODEN
- JLCRD
INIS
- Country of Publication
- United Kingdom
- Country of Input or Organization
- United Kingdom
- INIS RN
- 18084818
- Subject category
- S38: RADIATION CHEMISTRY, RADIOCHEMISTRY AND NUCLEAR CHEMISTRY;
- Descriptors DEI
- ALDEHYDES; CARBON 14 COMPOUNDS; CHEMICAL PREPARATION; DEHYDRATION; HYDROXY COMPOUNDS; LABELLING
- Descriptors DEC
- CARBON COMPOUNDS; ORGANIC COMPOUNDS; SYNTHESIS