Published June 1988 | Version v1
Journal article

Synthesis of [5-3H] hemimellitic acid

  • 1. Israel Atomic Energy Commission, Beersheba. Nuclear Research Center-Negev

Description

1,2,3-Benzenetricarboxylic acid (hemimellitic acid) tritiated in position 5 has been labelled at a specific activity of 16.2 Ci/mmol, starting from 3-bromo naphthalic anhydride. Attempts at direct bromination of the acid followed by tritiodebromination, or of general labelling by hydrogen-tritium exchange gave poor results. (author)

Additional details

Publishing Information

Journal Title
Journal of Labelled Compounds and Radiopharmaceuticals
Journal Volume
25
Journal Issue
6
Series
J. Labelled Compd. Radiopharm.
Journal Page Range
685-688
ISSN
0362-4803
CODEN
JLCRD

INIS

Country of Publication
United Kingdom
Country of Input or Organization
United Kingdom
INIS RN
20007650
Subject category
S38: RADIATION CHEMISTRY, RADIOCHEMISTRY AND NUCLEAR CHEMISTRY;
Descriptors DEI
AROMATICS; CARBOXYLIC ACIDS; CHEMICAL PREPARATION; LABELLING; TRITIUM COMPOUNDS
Descriptors DEC
HYDROGEN COMPOUNDS; ORGANIC ACIDS; ORGANIC COMPOUNDS; SYNTHESIS