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Haroun, N.A.; El-Masry, M.A.A.
Atomic Energy Establishment, Inshas (Egypt). Dept. of Metallurgy1980
Atomic Energy Establishment, Inshas (Egypt). Dept. of Metallurgy1980
AbstractAbstract
[en] The development of a process for coating alumina crucibles with MgO protective coat in a two-step slip casting operation is described. The best milling conditions for the alumina used were wet ball milling for 24 hr. MgO had to be calcined at 12000C to minimize hydration. Optimum slip casting conditions for alumina and magnesia were found to be L/S I and pH 3-6 or 9-II for the former, and L/S 3 (alcohol) and pH 8.5-10 for the latter. Sintering of Al2O3 and MgO in the temperature range 1150-5000C was investigated. Additions of NiO and MgO lowered the sintered densities at lower temperatures but improved the densification at 15000C. Near theoretical density Al2O3 and MgO crucibles were obtained. A two-step slip casting technique was developed to coat Al2O3 with MgO. Certain slow firing schedules could eliminate the otherwise observed coat-crucible separation and cracks. (author)
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1980; 17 p
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