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Sayre, E.V.; Harbottle, G.; Stoenner, R.W.; Otlet, R.L.; Evans, G.V.
Brookhaven National Lab., Upton, NY (USA); UKAEA Atomic Energy Research Establishment, Harwell. Low Level Measurements Lab1981
Brookhaven National Lab., Upton, NY (USA); UKAEA Atomic Energy Research Establishment, Harwell. Low Level Measurements Lab1981
AbstractAbstract
[en] Two recent developments are: the first is the mass-spectrometric separation of 14C and 12C ions, followed by counting of the 14C, while the second is the extension of conventional proportional counter operation, using CO2 as counting gas, to very small counters and samples. Although the second method is slow (months of counting time are required for 10 mg of carbon) it does not require operator intervention and many samples may be counted simultaneously. Also, it costs only a fraction of the capital expense of an accelerator installation. The development, construction and operation of suitable small counters are described, and results of three actual dating studies involving milligram scale carbon samples will be given. None of these could have been carried out if conventional, gram-sized samples had been needed. New installations, based on the use of these counters, are under construction or in the planning stages. These are located at Brookhaven Laboratory, the National Bureau of Standards (USA) and Harwell (UK). The Harwell installation, which is in advanced stages of construction, will be described in outline. The main significance of the small-counter method is, that although it will not suffice to measure the smallest (much less than 10 mg) or oldest samples, it will permit existing radiocarbon laboratories to extend their capability considerably, in the direction of smaller samples, at modest expense
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1981; 17 p; IAEA international symposium on methods of low-level counting and spectrometry; Berlin (Germany, F.R.); 6 - 10 Apr 1981; CONF-810409--4; Available from NTIS., PC A02/MF A01 as DE82004804
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