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Leisher, W.B.; Weissman, S.H.; Tallant, D.R.; Kubo, M.
Sandia National Labs., Albuquerque, NM (USA); Power Reactor and Nuclear Fuel Development Corp., Tokyo (Japan)1983
Sandia National Labs., Albuquerque, NM (USA); Power Reactor and Nuclear Fuel Development Corp., Tokyo (Japan)1983
AbstractAbstract
[en] We have developed a method to test powder leakage that has passed O-ring seals. To validate this method we have spiked a test fixture with 98 ng of U and recovered 130 +- 25 ng of U. We did not detect U at a detection limit of 26 ng in a fixture which was treated as a blank. This method has been applied to the leakage of UO2 powder passing the type of EPDM O-ring seals used in a SNM shipping cask belonging to PNC. Considering the three experimental tests in which no or very small quantities of U were detected as effective blank test, it appears that the level of external contamination is negligible. Therefore, we believe that the U quantities greater than 26 ng (6 tests) passed the primary O-ring seal. From this limited quantity of data, we observe no apparent correlation between the amount of U measured and either helium leak rate or equivalent tube diameter. The data for the 1300C tests indicate the possibility of a U/time relationship; however, more data are needed for verification
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1983; 10 p; 7. international symposium on packaging and transportation of radioactive materials; New Orleans, LA (USA); 15-20 May 1983; CONF-830528--38; Available from NTIS, PC A02/MF A01; 1 as DE83013773
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