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[en] Formation of ion complexes of f-elements with mixed heteropolymolybdatotungstates is determined. Compounds with the following composition: K13Eu(SiMo11O39)·H2O, K11M(PMoxW11-xO39)·H2O (where M=Eu, Nd, Pr, Yb) and Cs10Np(PMo11O39)2·pH2O - are precipitated out in the solid form. Characteristics of luminescence of the extracted solid complexes of Eu and Yb demonstrating, that during synthesis Mo:W initial ratio in the solution remains in solid phase, as well, are determined
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