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Edlund, M.; Heitland, P.; Visser, H.
Trends in sample preparation 2002. Development and application. Book of abstracts2002
Trends in sample preparation 2002. Development and application. Book of abstracts2002
AbstractAbstract
[en] Full text: The elemental analyses of soil and sewage sludge has developed to become one of the main applications for ICP optical emission spectrometry (ICP-OES) and is described in many official procedures. These methods include different acid mixtures and digestion techniques. Even though the German standard DIN 38414 part 7 and the Dutch NEN 6465 do not guarantee complete recoveries for all elements, they are widely accepted in Europe. This paper describes sample preparation, line selection and investigates precision, accuracy and Limits of detection. The SPECTRO CIROSCCD EOP with axial plasma observation and the SPECTRO CIROSCCD SOP with radial observation were compared and evaluated for the analyses of soil and sewage sludge. Accuracy was investigated using the certified reference materials CRM-141 R, CRM-143 R and GSD 11. Both instruments show excellent performance in terms of speed, precision, accuracy and detection limits for the determination of trace metals in soil and sewage sludge. (author)
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Wenzl, T.; Eberl, M.; Zischka, M.; Knapp, G. (eds.); Institute for Analytical Chemistry, Micro- and Radiochemistry, Graz University of Technology (Austria). Funding organisation: Agilent Technologies (Austria); Anton Paar GmbH (Austria); Berghof Laborprodukte GmbH (Germany); CEM International (Germany); Dionex GmbH (Germany); Graz University of Technology (Austria); Milestone Corporation (Italy); Personal Chemistry Company (Germany); Sigma Aldrich GmbH (Austria); Waters GmbH (Austria); 70 p; 2002; p. 51; TRISP 2002: Trends in sample preparation 2002; Seggau (Austria); 30 Jun - 3 Jul 2002; Available in abstract form only, full text entered in this record
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