Filters
Results 1 - 1 of 1
Results 1 - 1 of 1.
Search took: 0.033 seconds
AbstractAbstract
[en] The present investigation consists of two parts. The one part concerns the application of the Szilard-Chalmers effect in the separation of activities from neutron-irradiated biological material. The nuclides As-76, Au-198, Br-82, Ca-47, Cd-115, Cl-38, Co-60, Cr-51, Cs-134, Cu-64, Fe-59, Mg-27, Mo-99, Na-24, P-32, Rb-86, Se-75 and Zn-65 were extracted from either liver tissue, whole blood or muscle tissue. The extractions were made in water, 0.1 N HCl, 1 N HCl or conc. HCl respectively. The nuclides belonging to the alkali metals together with Br and Cl, were found present in the water and hydrochloric extracts to 96 per cent or more. In the conc. HCl extracts, the greater part of the nuclides were recovered to 90 per cent or more. The enrichment of the different nuclides obtained in the Szilard-Chalmers process was investigated as follows. After extraction of the nuclides from the irradiated material the solution obtained was divided into two parts, one of which was reactivated. The specific activities of the nuclides in the two solutions were then compared, thus giving the enrichment factor In one case, the residue of organic material after extraction was reactivated and the activity compared to the initial one. The effect of dilution together with the application of short irradiation periods favouring higher yield was investigated in the separation of Fe-59 from whole blood samples irradiated in frozen conditions. The other part of the investigation concerns an estimation of the amounts of the activities originating from polyethylene and quartz containers transferred to container surface due to the recoil effect in the thermal neutron-capture process, thus causing contamination of the sample. The universal range-energy relationship given by Lindhard and Scharff has been applied in these calculations. As regards containers with impurities in the ppm region, the amounts of activities transferred owing to this effect were found to be quite negligible. However, when the containers were rinsed with hydrochloric acid, activities were found to be extractable from a depth of the order of magnitude 10 and 10 cm in the polyethylene and the quartz materials respectively, which in some cases necessitates corrections
Primary Subject
Source
Jan 1965; 30 p; 34 refs., 8 tabs.
Record Type
Report
Report Number
Country of publication
ACTIVATION ANALYSIS, CHEMICAL ANALYSIS, CHEMISTRY, CHLORINE COMPOUNDS, HALOGEN COMPOUNDS, HOT ATOM CHEMISTRY, HYDROGEN COMPOUNDS, INORGANIC ACIDS, INORGANIC COMPOUNDS, MATERIALS, MINERALS, NONDESTRUCTIVE ANALYSIS, ORGANIC COMPOUNDS, ORGANIC POLYMERS, OXIDE MINERALS, POLYMERS, POLYOLEFINS, RADIOCHEMISTRY, SEPARATION PROCESSES
Reference NumberReference Number
INIS VolumeINIS Volume
INIS IssueINIS Issue