[en] Twenty seven representative samples were collected from two locations; Wadi Nugrus and Wadi Sikait, south Eastern Desert, Egypt. The area is characterized by abnormal radioactivity and has several archaeological sites (Sikait Temple). Emerald mining is a wide spread activity since Pharonic times at Sikait - Nugrus area. The concentration of the natural radionuclides (²³⁸U-series, ²³²Th-series and ⁴⁰K) are measured in all the rock samples by two techniques (HpGe detector and NaI(TI) detector). The Ra_eq, and H_ex for all samples are also determined. A comparative study between NaI and HpGe- detectors were carried out. The present work indicated that the equilibrium/disequilibrium ratios by using HpGe detector are more precise than that of Nal detectors. The radioactivity at Wadi Nugrus is higher than Wadi Sikait and also higher than the permissible level