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Martinez, L.G.; Orlando, M.T.D.; Rossi, J.L.; Passamai Junior, J.L.; Melo, F.C.L.; Ferreira, F.F., E-mail: lgallego@ipen.br
Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)2006
Instituto de Pesquisas Energeticas e Nucleares (IPEN/CNEN-SP), Sao Paulo, SP (Brazil)2006
AbstractAbstract
[en] Some phenomena in the field of condensed matter physics can be studied when the matter is submitted to extreme conditions of pressure, magnetic fields or temperatures. Once submitted to these conditions it is generally necessary to measure the properties of the matter in situ. The existence of a synchrotron light laboratory in Brazil opens up the chance of studying materials in extreme conditions by techniques like X-ray diffraction and absorption. However, when compared to high-energy synchrotrons accelerators, the Brazilian source offers a narrower energy range and lower flux. These facts impose limitation to perform diffraction experiments by energy dispersion and, consequently, the use of pressure cells with denser anvils like diamond. However, for a lower-pressure range, preliminary studies showed the viability of measurements in an angular dispersion configuration. This allows the use of silicon carbide anvils B4C. In this work it is described the development of a hydrostatic pressure cell suitable for X-rays diffraction measurements in the Brazilian Synchrotron Light Laboratory using materials and technologies developed by the institutions and researchers involved in this project (IPEN, UFES, CTA and LNLS). This development can provide the scientific community with the possibility of performing X-ray diffraction measurements under hydrostatic pressure, initially up to 2 GPa, with possibilities of increasing the maximum pressure to higher values, with or without application of magnetic fields and high or low temperatures. (author)
Original Title
Desenvolvimento de dispositivos para medidas de difracao de raios X com luz sincrotron em altas pressoes
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Source
2006; 8 p; 17. CBECIMAT: Brazilian congress on engineering and materials science; 17. CBECIMAT: Congresso brasileiro de engenharia e ciencia dos materiais; Foz do Iguacu, PR (Brazil); 15-19 Nov 2006; 21 refs, 4 figs. Code: 103-009.pdf
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Miscellaneous
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Conference
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BRAZILIAN ORGANIZATIONS, BREMSSTRAHLUNG, CHALCOGENIDES, CRYSTAL LATTICES, CRYSTAL STRUCTURE, ELECTROMAGNETIC RADIATION, ELEMENTS, MECHANICS, METALS, NATIONAL ORGANIZATIONS, OXIDES, OXYGEN COMPOUNDS, PRESSURE RANGE, PRESSURE RANGE MEGA PA, RADIATION SOURCES, RADIATIONS, REFRACTORY METAL COMPOUNDS, REFRACTORY METALS, RHENIUM COMPOUNDS, TRANSITION ELEMENT COMPOUNDS, TRANSITION ELEMENTS
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