[en] IPEN/CNEN-SP produces the fuel to supply its nuclear research reactor IEA-R1. The fuel is assembled with fuel plates containing an U₃Si₂-Al composite meat. A good homogeneity in the uranium distribution inside the fuel plate meat is important from the standpoint of irradiation performance. Considering the lower power of reactor IEA-R1, the uranium distribution in the fuel plate has been evaluated only by visual inspection of radiographs. However, with the possibility of IPEN to manufacture the fuel for the new Brazilian Multipurpose Reactor (RMB), with higher power, it urges to develop a methodology to determine quantitatively the uranium distribution into the fuel. This paper presents a methodology based on X-ray attenuation, in order to quantify the uranium concentration distribution in the meat of the fuel plate by using optical densities in radiographs and comparison with standards. The results demonstrated the inapplicability of the method, considering the current specification for the fuel plates due to the high intrinsic error to the method. However, the study of the errors involved in the methodology, seeking to increase their accuracy and precision, can enable the application of the method to qualify the final product. (author)