[en] The aim of this work is to improve radiation measurements of electromagnetic field (EMF) through realizing tests and calibrations of measurement devices by intercomparison within the microwaves (MW) range according to EMF wave cell properties. Actually, the calibration facility in electromagnetic field is not available in Syria; therefore, realizing an experimental system for electromagnetic field radiometer calibration is very important at national level. This study showed the possibility of using EMF wave cell in intercomparison of electromagnetic field radiometers in order to achieve a direct calibration via standard radiometer. The EMF wave cell properties were studied and the homogeneity of its EMF was tested using the EF Cube probe. Results showed that the field homogeneity inside the cell is good and the variation of electric field strength, within the comparison position, is less than 10% of measured values. It was recognized that the probe form and dimensions influence the comparison results; and measurement results showed that it's possible to achieve comparison in the working domain of EMF wave cell (10 - 3000 MHz) with a relative deviation of result values between 10% and 30% according to the measurement device and frequency range. Development of comparison process in order to obtain accurate results needs to improve mechanical supports of tested probes and to introduce a correction factor related to studied probe form and dimensions. From another side, it is better to carry out measurements at frequencies around the central frequency, and not close to frequency range borders, of the EMF wave cell working frequency domain. (author)