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Barbosa, A.S.; Santos, E.R.F.; Rodrigues, M.G.F.
Associacao Brasileira de Ceramica (ABC), Sao Paulo, SP (Brazil)2011
Associacao Brasileira de Ceramica (ABC), Sao Paulo, SP (Brazil)2011
AbstractAbstract
[en] The synthesis of MCM-22 is accomplished by hydrothermal treatment and long periods needed for crystallization, with the gradual growth of crystals of 10-14 days. MCM-22 catalyst is studied intensively as promising, with high thermal stability. As part of a line of research focused on the development of zeolite with lowest cost, this study aimed to examine the effect in decreasing the period of crystallization in the synthesis of zeolite MCM-22. The materials were characterized by X-ray diffraction (XRD) spectroscopy, X-ray Energy Dispersive (EDX) and Fourier transform infrared spectroscopy and Fourier transform (FT-IR). By XRD it was observed that the hydrothermal treatment used in the synthesis was effective during periods of crystallization and EDX was observed that the samples have a high percentage of silica and low alumina content, which gives them a high ratio SiO_2/Al_2O_3 characteristic of the MWW structure. (author)
Original Title
Estudo da influencia no periodo de cristalizacao na sintese da zeolita MCM-22
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2011; 11 p; 55. Brazilian congress on ceramics; 55. congresso brasileiro de ceramica; Porto de Galinhas, PE (Brazil); 29 May - 1 Jun 2011
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Miscellaneous
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Conference
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