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AbstractAbstract
[en] Oxide-dispersion strengthened ferritic steel was produced by high-energy attrition, leading to a complex nano-structure with deformed ferritic grains. After mechanical alloying, the powder was then consolidated by spark plasma sintering (SPS) using various thermo-mechanical treatments. Hot isostatic pressing (HIP) was also performed on the same powder for comparison. Above 1123 K (850 C), SPS consolidation-induced heterogeneous microstructure composed of ultrafine-grained regions surrounded by larger grains. Spatial distribution of the stored energy was measured in the bimodal microstructure using the Kernel average misorientation. In contrary to large recrystallized grains, ultra-fine grains are still sub-structured with low-angle grain boundaries. The precipitation kinetics of the nano-oxides during consolidation was determined by small-angle neutron scattering. Precipitation mainly occurred during the heating stage, leading to a high density of nano-clusters that are of prime importance for the mechanical properties. Other coarser titanium-enriched oxides were also detected. The multi-scale characterization allowed us to understand and model the evolution of the complex microstructure. An analytical evaluation of the contributing mechanisms explains the appearance of the complex grain structure and its thermal stability during further heat treatments. Inhomogeneous distribution of plastic deformation in the powder is the major cause of heterogeneous recrystallization and further grain growth during hot consolidation. Then, the thermal stability of coherent nano-oxides is responsible for effective grain boundary pinning in recovered regions where the driving pressure for recrystallization is lowered. This scenario is confirmed in both SPSed and HIPed materials. (authors)
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Available from doi: http://dx.doi.org/10.1007/s11661-013-2107-y; 54 refs.; Country of input: France
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Journal Article
Journal
Metallurgical and Materials Transactions. A, Physical Metallurgy and Materials Science; ISSN 1073-5623;
; v. 45A; p. 1485-1497

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