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AbstractAbstract
[en] In this work preparation of sulfonic acid functionalized magnetite encapsulated zirconia (Fe3O4@ZrO2-SO3H) has been reported. Structural, chemical, and magnetic properties of the magnetically supported catalyst have also been investigated by Fourier transform infrared (FT-IR) spectroscopy, wide angle X-ray diffraction spectroscopy (WXRD), thermal gravimetric analysis (TGA), energy dispersive X-ray analysis (EDX), transmission electron microscopy (TEM), vibrating sample magnetometer (VSM), Hammett acidity function and pH analysis as well as Brunauer-Emmett-Teller surface area measurement (SBET). The esterification reaction of various mono- and dicarboxylic acids with different alcohols was chosen to show the nano-catalytic activity. The reaction conditions were optimized and catalyst recovery was also demonstrated. The magnetic catalyst was magnetically separated and reused several times without significant loss of activity.
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Source
Available from http://jpst.irost.ir/article_651_9fccba4c6e57d1327c363d747aa1c4d4.pdf; This is an Open Access article distributed under the Creative Commons Attribution 4.0 License. (http://creativecommons.org/licenses/by/4.0/); Country of input: International Atomic Energy Agency (IAEA)
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Journal Article
Journal
Journal of Particle Science and Technology; ISSN 2423-4087;
; v. 4(1); p. 1-12

Country of publication
CHALCOGENIDES, CHEMICAL ANALYSIS, COHERENT SCATTERING, DIFFRACTION, ELECTROMAGNETIC RADIATION, ELECTRON MICROSCOPY, GRAVIMETRIC ANALYSIS, INTEGRAL TRANSFORMATIONS, IONIZING RADIATIONS, MAGNETOMETERS, MANAGEMENT, MEASURING INSTRUMENTS, MICROSCOPY, OXIDES, OXYGEN COMPOUNDS, PARTICLES, PHYSICAL PROPERTIES, PROCESSING, QUANTITATIVE CHEMICAL ANALYSIS, RADIATIONS, SCATTERING, SPECTRA, THERMAL ANALYSIS, TRANSFORMATIONS, TRANSITION ELEMENT COMPOUNDS, WASTE MANAGEMENT, WASTE PROCESSING, ZIRCONIUM COMPOUNDS
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