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Jacobsen, Saulo Davila; Hinrichs, Ruth; Blando, Eduardo; Vasconcellos, Marcos Antonio Zen; Figueroa, Carlos Alejandro; Aguzzoli, Cesar, E-mail: saulo_jacobsen@yahoo.com.br
Sociedade Brasileira de Pesquisa em Materiais (SBPMat), Rio de Janeiro, RJ (Brazil); Universidade Federal da Paraíba (UFPB), João Pessoa, PB (Brazil)2014
Sociedade Brasileira de Pesquisa em Materiais (SBPMat), Rio de Janeiro, RJ (Brazil); Universidade Federal da Paraíba (UFPB), João Pessoa, PB (Brazil)2014
AbstractAbstract
[en] Full text: The effect of different substrate temperatures and current densities on the wear behavior of plasma nitride H13 steel was analysed. The tribological properties were evaluated as a function of the phases formed in the near surface. The samples were DC nitrided for 5 h in a plasma with gas ratio of 80N2 /20H2 . The temperatures were 400, 430 and 480°C, and low and high current densities were used for each temperature. The formed phases were identified using Mössbauer spectroscopy and X-ray diffraction. Elemental depth distributions were determined with glow discharge optical emission spectroscopy. Coefficient of friction was determined with pin-on-disc tests that used the nitrided sample as the disc and Al2O3 sphere as the pin. Wear was evaluated with perfilometry. At 400°C only phase ε phase was observed at low current density while high density showed a mixture of ε, martensite and cementite. The wear rates were 1.4x10-8 and 1.2x10-8 mm3 /Nm, respectively. At 430°C ε-phase, martensite and cementite were observed for both samples, however a higher content of martensite was observed in the high current density sample. The wear rates of the samples nitrided in this temperature were 0.9x10-8 mm3 /Nm for low and 0.8x10-8 for high current density. At 480°C the ε- and γ´-phases and CrN were observed in the samples nitrided. At low current density the γ´-phase dominated and at high current density the ε-phase was dominant. Wear rates were 1.1x10-8 mm3 /Nm for both samples. Our results showed that lower wear rates correlated with higher contents of martensite and cementite. (author)
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Source
2014; 1 p; 13. Brazilian SBPMat meeting; Joao Pessoa, PB (Brazil); 28 Sep - 2 Oct 2014; Available in abstract form only; full text entered in this record
Record Type
Miscellaneous
Literature Type
Conference
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ALLOYS, ALUMINIUM COMPOUNDS, CARBON ADDITIONS, CHALCOGENIDES, COHERENT SCATTERING, DIFFRACTION, ELECTRIC DISCHARGES, GAMMA SPECTROMETERS, IRON ALLOYS, IRON BASE ALLOYS, MEASURING INSTRUMENTS, NITROGEN COMPOUNDS, OXIDES, OXYGEN COMPOUNDS, PNICTIDES, SCATTERING, SPECTROMETERS, TRANSITION ELEMENT ALLOYS
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