[en] This work presents an alternative and new procedure for the preparation of two-dimensional (2D) carbon particles. Carbon particles with 2D morphology with size from 10 to 60 μm were synthesized by a simple catalyst-free redox reaction at atmospheric pressure at temperatures in the range of 400 - 600 grad C. The aluminium powder with 2D particles was used as reactive template and oxidized by tetrachloromethane (CCl₄) and tetrachloroethylene (C₂Cl₄) for 60 min and 120 min. The carbon products reproduced the morphology of the original aluminium powder. The reaction also produced aluminium chloride (AlCl₃) as by-product, which was released from the reaction system in a gaseous state. According to BET and BJH analysis, carbon particles exhibit mesoporous structure with surface area in the range of 60 - 500 m² g^-: 1. In the case reaction of Al and CCl₄ SEM and TEM images show carbon particles with tiny 2D mesocrystalline structure in the size of 20 - 30 nm. At higher reaction temperatures as 600 grad C and 700 grad C, the formation of carbon materials with different morphologies, such as vermicular and one-dimensional (1D) carbon particles, was also observed. In the case reaction Al and C₂Cl₄ the carbon products was composed from different types of morphologies as carbon spheres, particles with 1D and 2D morphology. Carbon powder with 2D morphology which were prepared by CCl₄, were also tested as conductive additive in solid-state battery on the base Li-S. Battery with carbon powder as carbon conductive additive showed ≅ 17% capacity of maximal theoretical capacity of Li₂S battery, but battery displayed stable cycling stability until 90 cycles.