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Wlodarski, R.; Dembinski, W.; Przytycka, R.; Nowakowska, Z.
Institute of Nuclear Research, Warsaw (Poland)1974
Institute of Nuclear Research, Warsaw (Poland)1974
AbstractAbstract
[en] The studies on the production of sinterable uranium dioxide by means of precipiation of ammonium polyuranate with NH3 aq. from the aqueous uranyl nitrate solution and on its calcination and reduction with hydrogen were carried out. The influence of the precipiation parameters of ammonium polyuranate on its and uranium dioxide physico-chemical properties and their reproducibility as well as the possibilities to obtain these powders in the batch small scale process were examined. The physico-chemical properties of powders, impurities contents and the ability for pressing and sintering were determined. As a reult the most advantageous conditions of the precipitation has been established. It was found possible to obtain both ammonium polyuranate and uranium dioxide powders in a state o high purity with reproducible physico-chemical properties. The specific density of sintered pellets was higher than 94% of the theoretical density. (author)
Original Title
Prace nad otrzymywaniem w skali wielkolaboratoryjnej w procesie periodycznym ceramicznego dwutlenku uranu wedlug schematu technologicznego: azotan uranylu-poliuranian amonu-dwutlenek uranu
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Source
1974; 37 p
Record Type
Report
Report Number
Country of publication
ACTINIDE COMPOUNDS, AMMONIUM COMPOUNDS, CHALCOGENIDES, CHEMICAL ANALYSIS, CHEMICAL REACTIONS, CRYSTAL STRUCTURE, FABRICATION, GRAVIMETRIC ANALYSIS, HYDRIDES, HYDROGEN COMPOUNDS, MATERIALS WORKING, MICROSTRUCTURE, NITRATES, NITROGEN COMPOUNDS, NITROGEN HYDRIDES, OXIDES, OXYGEN COMPOUNDS, QUANTITATIVE CHEMICAL ANALYSIS, REDUCTION, THERMAL ANALYSIS, URANATES, URANIUM COMPOUNDS, URANIUM OXIDES, URANYL COMPOUNDS
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