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Karraker, D.G.; Stone, J.A.
Du Pont de Nemours (E.I.) and Co., Aiken, S.C. (USA). Savannah River Lab1977
Du Pont de Nemours (E.I.) and Co., Aiken, S.C. (USA). Savannah River Lab1977
AbstractAbstract
[en] Three Np(V) chlorocompounds, Cs3NpO2Cl4, ''Cs2NpO2Cl5,'' and ''(TPAs)2NpOCl5,'' where [TPAs+ = (C6H5)4As+], the tetraphenylarsonium cation, were studied to determine their Moessbauer spectra and magnetic properties. ''Cs2NpO2Cl5'' and ''(TPAs)2NpOCl5'' are of particular interest since the highly stable ONpO+ ion appeared to be partially chlorinated in strong HCl to a Cl2NpO+ ion. During the study, absorption and Moessbauer spectra indicated that ''Cs2NpOCl5'' and ''(TPAs)2NpOCl5'' were mainly mixtures of Np(IV) and Np(VI) chlorocompounds. To corroborate the spectral evidence, chlorocompounds of Np(IV) and Np(VI) were studied for comparison
Source
1977; 15 p; 29. annual southeastern regional meeting of the American Chemical Society; Tampa, FL, USA; 9 - 11 Nov 1977; CONF-771112--2; Available from NTIS., PC A02/MF A01
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