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Yamato, Aiji; Miyagawa, Naoto; Nomura, Tamotsu; Kinoshita, Mutsumi
Semi-annual progress report of Power Reactor and Nuclear Fuel Development Corporation, Tokai Works1976
Semi-annual progress report of Power Reactor and Nuclear Fuel Development Corporation, Tokai Works1976
AbstractAbstract
[en] Some methods for the analysis of I-129 in the environment are described. Iodide ion in seawater is coprecipitated with chloride ion by silver citrate powder, and that in seaweeds and in sediment is sublimated by heating at about 9000C in O2 atmosphere, and then the iodine is trapped in cooled NaOH and NaHSO3 mixed solution. The trapped iodine is precipitated with AgNO3 solution for γ-/X-ray spectrometry (detection limit asymptotically equals 30 pCi), or extracted into toluene scintillater solution for liquid scintillation counting. The decomposition of AgI is necessary for low level I-129 measurement; The AgI was transfered in a flask, added with 2N H2SO4 and Zn sand, and decomposed by stirring for 2 hr. Filtered the solution, added 0.5 g of NaNO2 and toluene scintillater to extract the iodine then added 1 ml of 2-methyl 1-butene to decolorize, the solution is measured by a liquid scintillation counter (detection limit asymptotically equals 1 pCi). This method can be applied for monitoring of low level radioactive water waste. (auth.)
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Source
Power Reactor and Nuclear Fuel Development Corp., Tokyo (Japan); p. 149-158; Sep 1976; p. 149-158
Record Type
Report
Literature Type
Progress Report
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BETA DECAY RADIOISOTOPES, BETA-MINUS DECAY RADIOISOTOPES, DAYS LIVING RADIOISOTOPES, HYDROGEN COMPOUNDS, INTERMEDIATE MASS NUCLEI, IODINE ISOTOPES, ISOTOPES, MEASURING INSTRUMENTS, MONITORING, NITRATES, NITROGEN COMPOUNDS, NUCLEI, ODD-EVEN NUCLEI, OXYGEN COMPOUNDS, RADIATION DETECTORS, RADIOISOTOPES, SILVER COMPOUNDS, SPECTRA, TRANSITION ELEMENT COMPOUNDS, WATER, YEARS LIVING RADIOISOTOPES
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