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AbstractAbstract
[en] An inert atmosphere box has been developed to work with sodium experimentally and analytically. The volumen of the box is 0.6 m3. A blower mounted inside the work chamber constantly circulates the argon from the work chamber through a gas purification system (nickel-catalyst 6525 and molecular sieve 4A). The flow rate is 450 l/h. The box is equipped with neoprene gloves. The glove ports can be closed with interior flanges. The work chamber is constantly kept to a low superpressure of 25 mm water gange. In a bypass the oxygen concentration is measured with the OXYLYT-electrolyte cell and the water vapour concentration with the KEIDEL-electrolytic hygrometer. During long-term operation oxygen levels of 35 vpm and water vapour levels of 50 vpm can be hold even when the gloves are not covered. By means of putting a vessel with liquid sodium in the work chamber oxygen levels of 8 vpm and water vapour levels of 20 vpm can be attained for short times. The inert atmosphere purity can be improved by means of increasing the gas flow rate. (author)
Original Title
Eine Schutzgasbox zur Handhabung von Natrium
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Secondary Subject
Source
Jan 1978; 12 p
Record Type
Report
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