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[en] This book give explanations on analytical chemistry with ten chapters, which deal with development of analytical chemistry, the theory of error with definition and classification, sample and treatment gravimetry on general process of gravimetry in aqueous solution and non-aqueous solution, precipitation titration about precipitation reaction and types, complexometry with summary and complex compound, oxidation-reduction equilibrium on electrode potential and potentiometric titration, solvent extraction and chromatograph and experiment with basic operation for chemical experiment.
[en] The special research is carried out on the leakage problem of the safety valve used in the field test. The main failure cause of safety valve has been found by dismantled them into parts, by checking the surfaces and the major dimensions, and analysis and inspection of the initial reason, measuring the coaxiality, then comparative tests for the relief valve, changing the parts, testing of airproof performance at cold state and hot state. According to this, the corresponding improvements has been taken to the 4 safety valve for repairing. The main cause of the problems that obtained and the improvements is accurate and appropriate from the testing results of the equipment and the submarine. According to the checkouts and tests results of products that hand over recently, the quality and the reliability of the safety valve has been improved evidently. (authors)
[en] Local mean velocity and turbulence intensity measurements were obtained with DANTEC 55 X two-dimensional Laser Dopper Anemometry (LDA) for rod bundle of reactor fuel assembly test model which was a 4 x 4 rod bundle. The data were obtained from different experimental cross-sections both upstream and downstream of the model support plate. Measurements performed at test Reynolds numbers of 1.8 x 104∼3.6 x 104. The results described the local and gross effects of the support plate on upstream and downstream flow distributions. A numerical computation was also given, the experimental results are in good agreement with the numerical one and the others in references. Finally, a few suggestions were proposed for how to use the LDA system well. (11 figs.)
[en] Highlights: • A new biodegradable poly(butylene succinate) (PBS)/poly(Z-L-lysine) (PZlys) composites were successfully prepared through physical blend. • PZlys may greatly affected the crystallization behaviors of PBS without changing its crystalline structure. • The degradation speed of PBS may be greatly accelerated by introduction of PZlys in PBS matrix. - Abstract: A new type of biodegradable poly(butylene succinate) (PBS)/poly(Z-L-lysine) (PZlys) composites were prepared. The crystallization behaviors were investigated by differential scanning calorimetry (DSC), wide angle X-ray diffraction (WAXD) and polarizing optical microscopy (POM) and the results showed that PZlys can restrict the crystallization of PBS, the crystallization speed of PBS/PZlys were slower than that of PBS, and the crystallization degree of the composites were smaller than that of PBS. However, the WAXD results showed that the incorporation of PZlys did not change the crystalline structure of PBS. The in vitro degradation experiments demonstrated that the degradation speed of the composites were faster than that of PBS. Moreover, the mechanical properties of the composites showed that the composites with a proper composition (for example, 80/20) can keep the mechanical properties of PBS without evident difference, which implied that the composites might be potentially useful as biodegradable materials
[en] Single molecule measurements have transformed our view of biomolecules. Owing to the ability of monitoring the activity of individual molecules, we now see them as uniquely structured, fluctuating molecules that stochastically transition between frequently many substrates, as two molecules do not follow precisely the same trajectory. Indeed, it is this discovery of critical yet short-lived substrates that were often missed in ensemble measurements that has perhaps contributed most to the better understanding of biomolecular functioning resulting from single molecule experiments. In this paper, we give a review on the three major techniques of single molecule force spectroscopy, and their applications especially in biology. The single molecular study of biotin-streptavidin interactions is introduced as a successful example. The problems and prospects of the single molecule force spectroscopy are discussed, too. (authors)