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Arena, Helene
Universite de Montpellier, 163 Rue Auguste Broussonnet, 34090 Montpellier (France); CEA DEN-DTCD (France)2016
Universite de Montpellier, 163 Rue Auguste Broussonnet, 34090 Montpellier (France); CEA DEN-DTCD (France)2016
AbstractAbstract
[en] This work takes place in the context of the long-term behavior of nuclear glasses under repository conditions. The main objective is to identify, understand and compare the effects of some chemical elements present in the glass composition and/or in the repository media (Zn, Mg, Ni, Co, Fe, Ca, Gd, Ce, K, Cs, Cr and Ag) on the processes involved in glass alteration by water. The cumulative or competitive nature of the effects of these chemical elements was determined. To reach this goal, a 6 oxides simple glass (ISG) has been altered for more than 500 days in a solution containing one or more of the chemical elements of interest. The results indicate that Zn, Mg, Ni, Co and Fe elements increase glass alteration forming secondary phases with the same structure and stoichiometry (tri-octahedral smectites). To form, these silicates consume chemical elements (Si, Al) from the environment and induce a pH decrease until a limiting value of pH. Beyond this pH the precipitation of secondary phases is inhibited and these chemical elements can be integrated into the gel, replacing Ca whose solubility increases at lower pH. As long as they form secondary phases, the effects of these elements are cumulative. Rare earths Gd and Ce also increase glass alteration forming secondary phases but their effects are lower as they contain less silicon. These elements are not integrated in the gel. Chromium increases glass alteration by precipitating with Ca and leading to a less protective gel, depleted in Ca. Silver precipitates as AgCl and has no effect on the alteration of the glass. The chemical elements K, Cs and Ca limit glass alteration by integrating into the gel and slowing down the transport phenomena therein. This integration is competitive: the order of integration (quantity and effectiveness glass alteration limitation) is the following Ca≥≥Cs≥K. Thus, the increase of glass alteration may be proportional to the quantity of elements promoting the precipitation of secondary phases, but the pH decrease limits the process. The effects of the elements that reduce glass alteration by incorporating into the gel are quantitatively limited by the gel composition and its ability to incorporate them, and qualitatively by the nature of the elements. (author)
[fr]
Cette these s'inscrit dans l'etude du comportement a long terme des verres nucleaires en conditions de stockage. Son objectif est de determiner, de comprendre et de comparer les effets de certains elements chimiques presents dans la composition du verre et/ou dans le milieu de stockage (Zn, Mg, Ni, Co, Fe, Ca, Gd, Ce, K, Cs, Cr et Ag) sur les differents processus mis en jeux lors de l'alteration aqueuse des verres nucleaires. Dans ce cadre, une attention particuliere a ete portee sur le caractere cumulatif ou competitif des effets de ces elements. Pour cela, un verre simple a 6 oxydes (ISG) a ete altere pendant plus de 500 jours dans une solution contenant un ou plusieurs des elements chimiques d'interet. Les elements Zn, Mg, Ni, Co et Fe augmentent l'alteration du verre en formant des phases secondaires de meme structure (smectites trioctaedriques) et de meme stoechiometrie (a l'element pres). Leur precipitation consomme des elements chimiques du milieu (Si, Al) et induit une diminution de pH. Ce processus se maintient jusqu'a l'atteinte d'un pH limite propre a chaque phase secondaire, au-dessous duquel leur precipitation est inhibee. Par la suite, ces elements peuvent s'integrer dans le gel d'alteration en remplacement du Ca rendu plus soluble par la baisse du pH. Tant qu'ils forment des phases secondaires, les effets de ces elements sont cumulatifs. Les terres rares Gd et Ce induisent une augmentation de l'alteration du verre en formant des phases secondaires, mais leurs effets sont plus faibles car les phases formees sont moins silicatees. Ces elements ne s'integrent pas dans le gel. Le Cr precipite avec le Ca pour former une phase qui appauvrit le gel en Ca, entraine une diminution du pH et augmente l'alteration du verre. Les elements K, Cs et Ca limitent l'alteration du verre en s'integrant dans le gel et en ralentissant les phenomenes de transport en son sein. Cette integration est competitive: l'ordre d'integration (quantite et efficacite sur la limitation de l'alteration) est le suivant Ca ≥≥ Cs ≥ K. L'element Ag precipitant sous forme d'AgCl, n'a pas d'effet sur l'alteration du verre: cette phase ne modifie ni le milieu, ni le developpement de la pellicule d'alteration. Ainsi, l'augmentation de l'alteration pourrait etre proportionnelle a la quantite d'elements favorisant la precipitation de phases secondaires, mais la diminution de pH qui l'accompagne limite ce processus. Les effets des elements qui diminuent l'alteration du verre en s'incorporant dans le gel, sont limites en quantite par la composition du gel et sa capacite a les recevoir, et en qualite par la nature meme des elementsOriginal Title
Effets cumulatifs et competitifs des elements chimiques sur l'alteration des verres nucleaires
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26 Feb 2016; 253 p; CEA-R--6450; 268 refs.; Available from the INIS Liaison Officer for France, see the 'INIS contacts' section of the INIS website for current contact and E-mail addresses: http://www.iaea.org/inis/Contacts/; Also available from Service commun de documentation Universite de Montpellier Place Eugene Bataillon, Bat 8 - CC 035, 34095 Montpellier Cedex 5 (France); Chimie et Physico-Chimie des Materiaux
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Tzounis, L.; Liebscher, M.; Stamm, M.; Mäder, E.; Pötschke, P.; Logothetidis, S., E-mail: ltzounis@physics.auth.gr, E-mail: logot@auth.gr2015
AbstractAbstract
[en] The thermoelectric properties of multi-wall carbon nanotube (MWCNT) -grafted glass fiber yarns (GF-CNT) and their epoxy model composites, as well as of polymer nanocomposites consisting of a polycarbonate (PC) matrix filled with differently functionalized MWCNTs have been examined. The GF-CNT hierarchical multi-scale structures were prepared by dip coating glass fiber yarns in a solution of carbonyl chloride modified MWCNTs; MWCNT-COCl (at a concentration of 0.5 mg/ml) under Ar atmosphere. The resulting GF-CNT exhibited high electrical conductivity (σ = 2.1×103 S/m) due to the dense MWCNT deposited networks. The fiber surface morphology was investigated by scanning electron microscopy (SEM). The GF-CNT showed Seebeck coefficient (S); S = 16.8 μV/K, and power factor (P.F); P.F = 0.59 μW/mK−2. The high electrical conductivity of the GF-CNT is a key parameter for an optimum thermoelectric performance, since it can facilitate the flow of the thermally induced charge carriers upon being exposed to a temperature gradient. Polycarbonate/MWCNT nanocomposites were prepared by small-scale melt-mixing process using a microcompounder. Unfunctionalized, carboxyl (-COOH) and hydroxyl (-OH) modified MWCNTs were incorporated in PC at a constant amount of 2.5 wt.%, concentration above the electrical percolation threshold. The amount of MWCNTs was kept low to understand the fundamental aspects of their physical properties and their correlation to the composite morphology, as revealed by transmission electron microscopy (TEM). It was found that different functional groups can affect the thermoelectric performance and the conductivity of the nanocomposites. Namely, the highest Seebeck coefficient (S) was found for the composite containing carboxyl functionalized MWCNTs (11.3 μV/K), due to the highest oxygen content of MWCNTs proven by X-Ray Photoelectron spectroscopy (XPS). It is believed that MWCNT-grafted glass fibers as reinforcements in composite structural materials and PC/MWCNT nanocomposites are ideal candidates for large-scale thermal energy harvesting. However, the thermoelectric values are still too low for commercial applications and in the future could be enhanced as will be discussed in this work
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NANOTEXNOLOGY 2014: International Conferences and Exhibition on Nanotechnologies and Organic Electronics; Thessaloniki (Greece); 5-12 Jul 2014; (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
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CARBON, CARBON COMPOUNDS, CARBONATES, CARBONIC ACID DERIVATIVES, COMPOSITE MATERIALS, DEPOSITION, ELECTRICAL PROPERTIES, ELECTRON MICROSCOPY, ELECTRON SPECTROSCOPY, ELEMENTS, MATERIALS, MICROSCOPY, NANOMATERIALS, NANOSTRUCTURES, NANOTUBES, NONMETALS, ORGANIC CHLORINE COMPOUNDS, ORGANIC COMPOUNDS, ORGANIC HALOGEN COMPOUNDS, ORGANIC OXYGEN COMPOUNDS, ORGANIC POLYMERS, OXYGEN COMPOUNDS, PHOTOELECTRON SPECTROSCOPY, PHYSICAL PROPERTIES, POLYMERS, SPECTROSCOPY, SURFACE COATING, TRANSPLANTS
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[en] This paper deals with modeling of the first damage mode, matrix micro-cracking, in helicopter rotor/wind turbine blades and how this effects the overall cross-sectional stiffness. The helicopter/wind turbine rotor system operates in a highly dynamic and unsteady environment leading to severe vibratory loads present in the system. Repeated exposure to this loading condition can induce damage in the composite rotor blades. These rotor/turbine blades are generally made of fiber-reinforced laminated composites and exhibit various competing modes of damage such as matrix micro-cracking, delamination, and fiber breakage. There is a need to study the behavior of the composite rotor system under various key damage modes in composite materials for developing Structural Health Monitoring (SHM) system. Each blade is modeled as a beam based on geometrically non-linear 3-D elasticity theory. Each blade thus splits into 2-D analyzes of cross-sections and non-linear 1-D analyzes along the beam reference curves. Two different tools are used here for complete 3-D analysis: VABS for 2-D cross-sectional analysis and GEBT for 1-D beam analysis. The physically-based failure models for matrix in compression and tension loading are used in the present work. Matrix cracking is detected using two failure criterion: Matrix Failure in Compression and Matrix Failure in Tension which are based on the recovered field. A strain variable is set which drives the damage variable for matrix cracking and this damage variable is used to estimate the reduced cross-sectional stiffness. The matrix micro-cracking is performed in two different approaches: (i) Element-wise, and (ii) Node-wise. The procedure presented in this paper is implemented in VABS as matrix micro-cracking modeling module. Three examples are presented to investigate the matrix failure model which illustrate the effect of matrix cracking on cross-sectional stiffness by varying the applied cyclic load
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ICNAAM-2014: International Conference on Numerical Analysis and Applied Mathematics 2014; Rhodes (Greece); 22-28 Sep 2014; (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
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Raguvarun, K.; Balasubramaniam, Krishnan; Rajagopal, Prabhu; Palanisamy, Suresh; Nagarajah, Romesh; Kapoor, Ajay; Hoye, Nicholas; Curiri, Dominic, E-mail: prajagopal@iitm.ac.in, E-mail: prajagopal@iitm.ac.in, E-mail: prajagopal@iitm.ac.in2015
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[en] Additive manufacturing methods are gaining increasing popularity for rapidly and efficiently manufacturing parts and components in the industrial context, as well as for domestic applications. However, except when used for prototyping or rapid visualization of components, industries are concerned with the load carrying capacity and strength achievable by additive manufactured parts. In this paper, the wire-arc additive manufacturing (AM) process based on gas tungsten arc welding (GTAW) has been examined for the internal structure and constitution of components generated by the process. High-resolution 3D X-ray tomography is used to gain cut-views through wedge-shaped parts created using this GTAW additive manufacturing process with titanium alloy materials. In this work, two different control conditions for the GTAW process are considered. The studies reveal clusters of porosities, located in periodic spatial intervals along the sample cross-section. Such internal defects can have a detrimental effect on the strength of the resulting AM components, as shown in destructive testing studies. Closer examination of this phenomenon shows that defect clusters are preferentially located at GTAW traversal path intervals. These results highlight the strong need for enhanced control of process parameters in ensuring components with minimal defects and higher strength
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41. Annual Review of Progress in Quantitative Nondestructive Evaluation; Boise, ID (United States); 20-25 Jul 2014; (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
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Suter, J. D.; Ramuhalli, P.; Hu, S.; Li, Y.; Jiang, W.; Edwards, D. J.; Schemer-Kohrn, A. L.; Johnson, B. R.; McCloy, J. S.; Xu, K., E-mail: pradeep.ramuhalli@pnnl.gov, E-mail: pradeep.ramuhalli@pnnl.gov, E-mail: john.mccloy@wsu.edu, E-mail: john.mccloy@wsu.edu2015
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[en] Verifying the structural integrity of passive components in light water and advanced reactors will be necessary to ensure safe, long-term operations of the existing U.S. nuclear fleet. This objective can be achieved through nondestructive condition monitoring techniques, which can be integrated with plant operations to quantify the “state of health” of structural materials in real-time. While nondestructive methods for monitoring many classes of degradation (such as fatigue or stress corrosion cracking) are relatively advanced, this is not the case for degradation caused by irradiation. The development of nondestructive evaluation technologies for these types of degradation will require advanced materials characterization techniques and tools that enable comprehensive understanding of nuclear reactor material microstructural and behavioral changes under extreme operating environments. Irradiation-induced degradation of reactor steels causes changes in their microstructure that impacts their micro-magnetic properties. In this paper, we describe preliminary results of integrating advanced material characterization techniques with meso-scale computational models. In the future, this will help to provide an interpretive understanding of the state of degradation in structural materials. Microstructural data are presented from monocrystalline Fe and are correlated with variable-field magnetic force microscopy and micro-magnetic measurements. Ongoing research is focused on extending the measurements and models on thin films to gain insights into the structural state of irradiated materials and the resulting impact on magnetic properties. Preliminary conclusions from these correlations are presented, and next steps described
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41. Annual Review of Progress in Quantitative Nondestructive Evaluation; Boise, ID (United States); 20-25 Jul 2014; (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
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Ewert, Uwe; Redmer, Bernhard; Walter, David; Thiessenhusen, Kai-Uwe; Bellon, Carsten; Nicholson, P. Ian; Clarke, Alan L.; Finke-Härkönen, Klaus-Peter, E-mail: uwe.ewert@bam.de, E-mail: uwe.ewert@bam.de, E-mail: uwe.ewert@bam.de, E-mail: uwe.ewert@bam.de, E-mail: uwe.ewert@bam.de, E-mail: ian.nicholson@twi.co.uk, E-mail: klaus.harkonen@ajat.fi2015
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[en] The new standard 'ISO 17636-2:2013: Non-destructive testing of welds - Radiographic testing - Part 2: X- and gamma-ray techniques with digital detectors', defines the practice for radiographic inspection of welded pipes for manufacturing and in-service inspection. It is applied in Europe for inspections of pipe welds in nuclear power plants as well as in chemical plants and allows a faster inspection with digital detector arrays (DDA) than with film. Nevertheless, it does not allow the evaluation of the depth and shape of volumetric and planar indications. In 2001 a planar tomography scanner, TomoCAR, was introduced for mechanized radiographic testing (RT) inspection and non-destructive measurement of cross sections. The project TomoWELD is based on a new concept of the scan geometry, an enhanced GPU based reconstruction, and the application of a new generation of photon counting DDAs based on CdTe crystal CMOS hybrids. The new detector permits the selection of energy thresholds to obtain an optimum energy range and reduction of the influence of scattered radiation. The concept and first measurements are presented. Flaw depth and shape of volumetric and planar irregularities can be determined
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41. Annual Review of Progress in Quantitative Nondestructive Evaluation; Boise, ID (United States); 20-25 Jul 2014; (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
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BOSONS, CADMIUM COMPOUNDS, CHALCOGENIDES, DIAGNOSTIC TECHNIQUES, DIMENSIONS, ELECTROMAGNETIC RADIATION, ELEMENTARY PARTICLES, FILMS, INDUSTRIAL PLANTS, INSPECTION, IONIZING RADIATIONS, JOINTS, MASSLESS PARTICLES, NUCLEAR FACILITIES, POWER PLANTS, RADIATIONS, TELLURIDES, TELLURIUM COMPOUNDS, THERMAL POWER PLANTS, TOMOGRAPHY
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[en] In order to understand the importance of the retrogression and re-aging as a heat treatment for improving microstructural and mechanical properties of the Al-Zn-Mg-Cu powder metallurgy alloys, Al-Zn-Mg-Cu-Fe-Cr alloys were fabricated from the elemental powders. Green compacts are compressed under compaction pressure about 370 MPa. The sintering process carried out for the samples of aluminum alloys at temperature was 650°C under argon atmosphere for two hours. The sintered compacts were subjected into homogenizing condition at 470°C for 1.5 hours and then aged at 120°C for 24 hours (T6 temper) after that it carried out the retrogressed at 180°C for 30 min., and then re-aged at 120°C for 24 hours (RRA). Observations microstructures were examined using optical, scanning electron microscopy coupled with energy dispersive spectroscopy and X-ray diffraction. Density and porosity content was conducted for the samples of alloys. The result showing that the highest Vickers hardness exhibited for an Al-Zn-Mg-Cu alloy after underwent the retrogression and reaging treatment. Increasing in hardness was because of the precipitation hardening through precipitate the (Mg Zn) and (Mg2Zn11) phases during matrix of aluminum-alloy
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ICoMEIA 2014: International Conference on Mathematics, Engineering and Industrial Applications 2014; Penang (Malaysia); 28-30 May 2014; (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
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[en] Superhydrophobic surfaces with contact angle (CA) >150 and sliding angle (SA) <10 have been aroused curiosity over the years due to their various applications. Superhydrophobicity can be obtained tailoring the chemistry and the roughness of the surface, mimicking the Lotus flower. Most superhydrophobic surfaces based on secondary bonding lose their roughness in harsh conditions and are unsuitable for practical applications. Photoreactive SiO2 nanoparticles (NPs) based on benzophenone (BP) can be a very effective tool for formation of reactive species that function as a molecular bridge by covalent bonding between the NP and any polymer matrix with C-C and C-H bonds. The present work focused on thermoset radiation curing urethane acrylate. Upon UV irradiation reactive excited nπ* triplet benzophenone species are formed and react through hydrogen abstraction to form ketyl radicals which interact with a radicals from the UV irradiated polymer matrix to yield covalent bonding. Roughness was achieved by dipping the substrate in SiO2@BPs NPs dispersion followed by irradiation. Fluoroalkylsilane was used to obtain hydrophobic top layer. AFM nano manipulation was used to verify the immobilization of NPs. Evaluation of durability was made using air flow at 300 km/hr. Preliminary results indicate the formation of super hydrophobic surfaces (CA>150 and SA<10) with improved stability
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PPS-30: 30. International Conference of the Polymer Processing Society; Cleveland, OH (United States); 6-12 Jun 2014; (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
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BORON COMPOUNDS, CARBAMATES, CARBONIC ACID DERIVATIVES, CARBOXYLIC ACID SALTS, CHALCOGENIDES, CHEMICAL RADIATION EFFECTS, CURING, ELECTROMAGNETIC RADIATION, FABRICATION, JOINING, LIFETIME, MATERIALS, MECHANICAL PROPERTIES, MICROSCOPY, MINERALS, ORGANIC COMPOUNDS, ORGANIC NITROGEN COMPOUNDS, OXIDE MINERALS, OXIDES, OXYGEN COMPOUNDS, PARTICLES, PHOSPHIDES, PHOSPHORUS COMPOUNDS, PNICTIDES, POLYMERS, RADIATION EFFECTS, RADIATIONS, SILICON COMPOUNDS, SURFACE PROPERTIES
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[en] Micro structured optical plastics components are intensively used i. e. in consumer electronics, for optical sensors in metrology, innovative LED-lighting or laser technology. Injection moulding has proven to be successful for the large-scale production of those parts. However, the production of those parts still causes difficulties due to challenges in the moulding and demoulding of plastics parts created with laser structured mould inserts. A complete moulding of the structures often leads to increased demoulding forces, which then cause a breaking of the structures and a clogging of the mould. An innovative approach is to combine PVD-coated (physical vapour deposition), laser structured inserts and a variothermal moulding process to create functional mic8iüro structures in a one-step process. Therefore, a PVD-coating is applied after the laser structuring process in order to improve the wear resistance and the anti-adhesive properties against the plastics melt. In a series of moulding trials with polycarbonate (PC) and polymethylmethacrylate (PMMA) using different coated moulds, the mould temperature during injection was varied in the range of the glass transition and the melt temperature of the polymers. Subsequently, the surface topography of the moulded parts is evaluated by digital 3D laser-scanning microscopy. The influence of the moulding parameters and the coating of the mould insert on the moulding accuracy and the demoulding behaviour are being analysed. It is shown that micro structures created by ultra-short pulse laser ablation can be successfully replicated in a variothermal moulding process. Due to the mould coating, significant improvements could be achieved in producing micro structured optical plastics components
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PPS-30: 30. International Conference of the Polymer Processing Society; Cleveland, OH (United States); 6-12 Jun 2014; (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
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[en] We investigated the efficient use of cellulose to resolve the problem of the depletion of fossil resources. In this study, as the biomass material, the green composite based on natural rubber (NR) and the flake-shaped cellulose particles (FSCP) was produced. In order to further improvement of functional characteristics, epoxidized natural rubber (ENR) was also used instead of NR. The FSCP were produced by mechanical milling in a planetary ball mill with a grinding aid as a cellulose aggregation inhibitor. Moreover, talc and mica particles were used to compare with FSCP. NR and ENR was mixed with vulcanizing agents and then each filler was added to NR compound in an internal mixer. The vulcanizing agents are as follows: stearic acid, zinc oxide, sulfur, and vulcanization accelerator. The functionalities of the composites were evaluated by a vibration-damping experiment and a gas permeability experiment. As a result, we found that FSCP filler has effects similar to (or more than) inorganic filler in vibration-damping and O2 barrier properties. And then, vibration- damping and O2 barrier properties of the composite including FSCP was increased with use of ENR. In particular, we found that ENR-50 composite containing 50 phr FSCP has three times as high vibration-damping property as ENR-50 without FSCP
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PPS-30: 30. International Conference of the Polymer Processing Society; Cleveland, OH (United States); 6-12 Jun 2014; (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA)
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CARBOHYDRATES, CARBOXYLIC ACIDS, CHALCOGENIDES, COMMINUTION, ELASTOMERS, ELEMENTS, ENERGY SOURCES, EVALUATION, MACHINING, MATERIALS, MINERALS, MONOCARBOXYLIC ACIDS, NONMETALS, ORGANIC ACIDS, ORGANIC COMPOUNDS, ORGANIC POLYMERS, OXIDES, OXYGEN COMPOUNDS, PHYSICAL PROPERTIES, POLYMERS, POLYSACCHARIDES, RENEWABLE ENERGY SOURCES, RUBBERS, SACCHARIDES, SILICATE MINERALS, ZINC COMPOUNDS
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