Published March 2014
| Version v1
Book
Quantification and isotope ratio measurement of boron by ICP-TOF-MS after its pyrohydrolytic extraction from U3Si2-Al fuel
- 1. Radioanalytical Chemistry Div., Bhabha Atomic Research Centre, Mumbai (India)
Description
A novel and reagent free quantitative separation procedure based on pyrohydrolysis technique was developed for quantitative recovery of B from U3Si2-Al matrix followed by its analysis employing ICP-MS. The method for B determination was validated by an independent spectrophotometric technique. The developed method was applied successfully for the analysis of three U3Si2-Al samples. The CAIS technique was applied for correcting the mass bias on B isotope ratio measurement thereby improving the precision to 0.2% RSD
Additional details
Publishing Information
- Publisher
- Indian Society for Mass Spectrometry
- Imprint Place
- Mumbai (India)
- ISBN
- 978-81-904442-6-2
- Imprint Title
- Proceedings of the twenty eighth ISMAS symposium cum workshop on mass spectrometry
- Imprint Pagination
- 352 p.
- Journal Page Range
- p. 212-215
Conference
- Title
- 28. ISMAS symposium cum workshop on mass spectrometry
- Acronym
- ISMAS-WS-2014
- Dates
- 9-13 Mar 2014
- Place
- Parwanoo (India)
INIS
- Country of Publication
- India
- Country of Input or Organization
- India
- INIS RN
- 45077570
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Resource subtype / Literary indicator
- Conference
- Descriptors DEI
- BORON 10; BORON 11; ICP MASS SPECTROSCOPY; ISOTOPE RATIO; SILICIDES; SPECTROPHOTOMETRY; URANIUM COMPOUNDS
- Descriptors DEC
- ACTINIDE COMPOUNDS; BORON ISOTOPES; DIMENSIONLESS NUMBERS; ISOTOPES; LIGHT NUCLEI; MASS SPECTROSCOPY; NUCLEI; ODD-EVEN NUCLEI; ODD-ODD NUCLEI; SILICON COMPOUNDS; SPECTROSCOPY; STABLE ISOTOPES
Optional Information
- Notes
- 10 refs., 2 figs., 2 tabs.